Extraction and evaporation recrystallization essay

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Extraction and evaporation recrystallization essay

Zinc oxide can be called a multifunctional material thanks to its unique physical and chemical properties. The first part of this paper presents the most important methods of preparation of ZnO divided into metallurgical and chemical methods.

The mechanochemical process, controlled precipitation, sol-gel method, solvothermal and hydrothermal method, method using emulsion and microemulsion enviroment and other methods of obtaining zinc oxide were classified as chemical methods. In the next part of this review, the modification methods of ZnO were characterized.

The modification with organic carboxylic acid, silanes and inroganic metal oxides compounds, and polymer matrices were mainly described. Finally, we present possible applications in various branches of industry: This review provides useful information for specialist dealings with zinc oxide.

Introduction Zinc oxide, with its unique physical and chemical properties, such as high chemical stability, high electrochemical coupling coefficient, broad range of radiation absorption and high photostability, is a multifunctional material [ 12 ].

In materials science, zinc oxide is classified as a semiconductor in group II-VI, whose covalence is on the boundary between ionic and covalent semiconductors. A broad energy band 3.

Extraction and evaporation recrystallization essay

The piezo- and pyroelectric properties of ZnO mean that it can be used as a sensor, converter, energy generator and photocatalyst in hydrogen production [ 56 ]. Because of its hardness, rigidity and piezoelectric constant it is an important material in the ceramics industry, while its low toxicity, biocompatibility and biodegradability make it a material of interest for biomedicine and in pro-ecological systems [ 7 — 9 ].

The variety of structures of nanometric zinc oxide means that ZnO can be classified among new materials with potential applications in many fields of nanotechnology.

Zinc oxide can occur in one- 1Dtwo- 2Dand three-dimensional 3D structures. One-dimensional structures make up the largest group, including nanorods [ 10 — 12 ], -needles [ 13 ], -helixes, -springs and -rings [ 14 ], -ribbons [ 15 ], -tubes [ 16 — 18 ] -belts [ 19 ], -wires [ 20 — 22 ] and -combs [ 23 ].

Examples of 3D structures of zinc oxide include flower, dandelion, snowflakes, coniferous urchin-like, etc. ZnO provides one of the greatest assortments of varied particle structures among all known materials see Figure 1.

In this review, the methods of synthesis, modification and application of zinc oxide will be discussed.

The zinc oxide occurs in a very rich variety of structures and offers a wide range of properties. The variety of methods for ZnO production, such as vapour deposition, precipitation in water solution, hydrothermal synthesis, the sol-gel process, precipitation from microemulsions and mechanochemical processes, makes it possible to obtain products with particles differing in shape, size and spatial structure.

These methods are described in detail in the following sections Table 1. Metallurgical Process Metallurgical processes for obtaining zinc oxide are based on the roasting of zinc ore. According to the ISO standard [ 68 ], zinc oxide is classified either as type A, obtained by a direct process the American process ; or type B, obtained by an indirect process the French process.

The direct American process involves the reduction of zinc ore by heating with coal such as anthracitefollowed by the oxidation of zinc vapour in the same reactor, in a single production cycle.

This process was developed by Samuel Wetherill, and takes place in a furnace in which the first layer consists of a coal bed, lit by the heat remaining from the previous charge. Above this bed is a second layer in the form of zinc ore mixed with coal.Recrystallization was done to remove impurities from the sample.

The percent recovery of benzoic acid during recrystallization is %. The difference between the pure and impure samples was observed by comparison of melting points.

It was found that impure sample had a lower and wider melting point range of (C). 1. Introduction. Zinc oxide, with its unique physical and chemical properties, such as high chemical stability, high electrochemical coupling coefficient, broad range of radiation absorption and high photostability, is a multifunctional material [1,2].In materials science, zinc oxide is classified as a semiconductor in group II-VI, whose covalence is on the boundary between ionic and covalent.

Crystallization is the (natural or artificial) process by which a solid forms, where the atoms or molecules are highly organized into a structure known as a grupobittia.com of the ways by which crystals form are precipitating from a solution, freezing, or more rarely deposition directly from a grupobittia.comutes of the resulting crystal depend largely on factors such as .

The purpose of this lab is to isolate trimyristin from nutmeg by performing a simple solid-liquid extraction and to purify the trymyristin using the method of recrystallization.

Procedure: Place 5 g of nutmeg and 50 mL of DCM into a mL round bottom flask, and reflux the mixture for 30 minutes. Experiment 1 A. Extraction and Recrystallization B. Thin Layer Chromatography (TLC) Lut Ming Cheng, , CHM, Section C TA: Wendy Campbell Due Date: September 22, 1 – Theory and Mechanism In order to separate a mixture of organic components, extraction and recrystallization techniques are used to achieve the goal.

The Preparation of Aspirin, the Recrystallisation of Aspirin and the Melting Point Determination of Aspirin. Results At the end of the experiment, the result gotten should be a result of 40 – 60 % yield and a melting point that is around the theoretical melting point of aspirin, which is °C – °C.

Extraction and evaporation recrystallization essay
Crystallization - Wikipedia